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乙二醇
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63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87243-93-4
合成路线
（共 15 条）
87243-93-4
→
反应条件
18874-22-1
反应条件
thionyl chloride in dichloromethane T=26°C; 24 h;
参考文献
Keglevich, Gyoergy; Kiss, Nora Zsuzsa; Koertvelyesi, Tamas
Heteroatom Chemistry, 2013 , vol. 24, # 2 p. 91 - 99
100-51-6
苯甲醇
+
87243-93-4
→
反应条件
2921-67-7
反应条件
1: 1-hydroxy-3-methyl-2,5-dihydro-1H-phosphole 1-oxide With 1-propanephosphonic acid cyclic anhydride in ethyl acetate 0.166667 h; Green chemistry; 2: benzyl alcohol in ethyl acetate T=25°C; 0.5 h; Green chemistry;
参考文献
Jablonkai, Erzsebet; Milen, Matyas; Drahos, Laszlo; Keglevich, Gyoergy
Tetrahedron Letters, 2013 , vol. 54, # 44 p. 5873 - 5875
100-39-0
溴化苄
+
87243-93-4
→
反应条件
2921-67-7
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate T=100°C; P=1500.15 - 2250.23 Torr; 1 h; Microwave irradiation;
参考文献
Balint, Erika; Jablonkai, Erzsebet; Balint, Maria; Keglevich, Gyoergy
Heteroatom Chemistry, 2010 , vol. 21, # 4 p. 211 - 214
100-44-7
苄基氯
+
87243-93-4
→
反应条件
2921-67-7
反应条件
potassium carbonate T=100°C; Microwave irradiation;
参考文献
Keglevich, Gyoergy; Kiss, Nora Z.; Balint, Erika; Jablonkai, Erzsebet; Gruen, Alajos; Milen, Matyas; Frigyes, David; Gre, Istvan
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 4 p. 802 - 803
71-41-0
正戊醇
+
87243-93-4
→
反应条件
2921-66-6
反应条件
T=220°C; 2.5 h; Sealed tubeMicrowave irradiation;
参考文献
Jablonkai, Erzsebet; Milen, Matyas; Drahos, Laszlo; Keglevich, Gyoergy
Tetrahedron Letters, 2013 , vol. 54, # 44 p. 5873 - 5875
67-63-0
异丙醇
+
87243-93-4
→
反应条件
3105-69-9
反应条件
1: 1-hydroxy-3-methyl-2,5-dihydro-1H-phosphole 1-oxide With 1-propanephosphonic acid cyclic anhydride in ethyl acetate 0.166667 h; Green chemistry; 2: isopropyl alcohol in ethyl acetate T=25°C; 3 h; Green chemistry;
参考文献
Jablonkai, Erzsebet; Milen, Matyas; Drahos, Laszlo; Keglevich, Gyoergy
Tetrahedron Letters, 2013 , vol. 54, # 44 p. 5873 - 5875
75-26-3
2-溴丙烷
+
87243-93-4
→
反应条件
3105-69-9
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate T=100°C; P=1500.15 - 2250.23 Torr; 1 h; Microwave irradiation;
参考文献
Balint, Erika; Jablonkai, Erzsebet; Balint, Maria; Keglevich, Gyoergy
Heteroatom Chemistry, 2010 , vol. 21, # 4 p. 211 - 214
87243-93-4
→
反应条件
183163-62-4
反应条件
1: 1.) SOCl2, 2.) HSiCl3 3: t-BuOOH 4: Br2 5: HSiCl3 6: Et3N View Scheme
参考文献
Quin, Louis D.; Ionkin, Alexey S.; Kalgutkar, Rajdeep; Keglevich, Gyoergy
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 433 - 436
67-56-1
甲醇
+
87243-93-4
→
反应条件
695-59-0
反应条件
1: 1-hydroxy-3-methyl-2,5-dihydro-1H-phosphole 1-oxide With 1-propanephosphonic acid cyclic anhydride in ethyl acetate 0.166667 h; Green chemistry; 2: methanol in ethyl acetate T=25°C; 0.5 h; Green chemistry;
参考文献
Jablonkai, Erzsebet; Milen, Matyas; Drahos, Laszlo; Keglevich, Gyoergy
Tetrahedron Letters, 2013 , vol. 54, # 44 p. 5873 - 5875
87243-93-4
→
反应条件
7529-24-0
反应条件
1: thionyl chloride / chloroform; tetrahydrofuran 2: tetrahydrofuran / 0 - 26 °C View Scheme
参考文献
Bagi, Peter; Kovacs, Tamara; Szilvasi, Tibor; Pongracz, Peter; Kollar, Laszlo; Drahos, Laszlo; Fogassy, Elemer; Keglevich, Gyoergy
Journal of Organometallic Chemistry, 2014 , vol. 751, p. 306 - 313
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