反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 40 °C
2: sodium tetrahydroborate / methanol / 1.5 h / 0 - 20 °C / |Inert atmosphere
3: sodium azide / N,N-dimethyl-formamide / 70 °C
View Scheme
参考文献
Liao, Longyan; Liu, Jenny; Dreaden, Erik C.; Morton, Stephen W.; Shopsowitz, Kevin E.; Hammond, Paula T.; Johnson, Jeremiah A.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5896 - 5899