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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
872595-54-5
合成路线
（共 5 条）
105290-13-9
→
反应条件
872595-54-5
反应条件
selenium(IV) oxide in xylene 24 h; Heating;
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
90-33-5
4-甲基伞形酮
→
反应条件
872595-54-5
反应条件
1: 80 percent / K2CO3; KI / acetone / Heating 2: 95 percent / aq. NaOH / 3 h / Heating 3: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / Pd/C / toluene / 6 h / Heating 4: 90 percent / SeO2 / xylene / 24 h / Heating View Scheme
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
73207-85-9
4-甲基-6,7,8,9-四氢-[1]苯并呋喃并[3,2-g]苯并吡喃-2-酮
→
反应条件
872595-54-5
反应条件
1: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / Pd/C / toluene / 6 h / Heating 2: 90 percent / SeO2 / xylene / 24 h / Heating View Scheme
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
86048-54-6
4-甲基-7-(2-氧代环己基氧基)-色烯-2-酮
→
反应条件
872595-54-5
反应条件
1: 95 percent / aq. NaOH / 3 h / Heating 2: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / Pd/C / toluene / 6 h / Heating 3: 90 percent / SeO2 / xylene / 24 h / Heating View Scheme
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
108-46-3
间苯二酚
→
反应条件
872595-54-5
反应条件
1: 80 percent / H2SO4 / 0 - 5 °C 2: 80 percent / K2CO3; KI / acetone / Heating 3: 95 percent / aq. NaOH / 3 h / Heating 4: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / Pd/C / toluene / 6 h / Heating 5: 90 percent / SeO2 / xylene / 24 h / Heating View Scheme
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
