1: 5,6-dibromohexan-1-ol With potassium hydroxide in diethyl ether
Heating;
2: methanesulfonyl chloride With triethylamine in dichloromethane
T=20°C;
3: With lithium bromide in 1-methyl-pyrrolidin-2-one
T=20°C; Title compound not separated from byproducts;
参考文献
Diez-Gonzalez, Silvia; Blanco, Luis
Journal of Organometallic Chemistry, 2006 , vol. 691, # 26 p. 5531 - 5539
