反应条件
in toluene byproducts: Me2SnCl2; (Ar); using Schlenk techniques; vac. transferring of toluene into flask with C12H8SnMe2 at -78°C; addn. dropwise via syringe of soln. of C6H5BCl2 at -78°C, slowly warming to room temp., stirring overnight; removal of solvent under vac., transferring to a sublimator, removal of Me2SnCl2 under static vac. at 40°C for 2 days, elem. anal.;
参考文献
Romero, Patricio E.; Piers, Warren E.; Decker, Stephen A.; Chau, Dan; Woo, Tom K.; Parvez, Masood
Organometallics, 2003 , vol. 22, # 6 p. 1266 - 1274
