in octane boroxine was added under Ar to a soln. of AlCl3, the mixt was heated at about 100 °C for 10 h (stirring);; filtration, residue washed with hexane, dried in vac. at 20°C, recrystd. from benzene; elem. anal.;;
参考文献
Koester, Roland; Angermund, Klaus; Serwatowski, Janusz; Sporzynski, Andrzej
Chemische Berichte, 1986 , vol. 119, # 4 p. 1301 - 1314
