tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; dimethyl sulfoxide
T=20°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Baeckvall,J.E.; Nystroem,J.E.; Norberg,R.
Journal of the American Chemical Society, 1985 , vol. 107, p. 3676
1: With copper(l) iodide in DMF (N,N-dimethyl-formamide)
T=120°C; 40 h;
2: With sodium hydrogencarbonate in DMF (N,N-dimethyl-formamide); dichloromethane; water
T=20°C;
参考文献
GLAXO GROUP LIMITED
Patent: WO2005/26125 A1, 2005 ;
Location in patent: Page/Page column 20 ;
WO 2005/026125 A1