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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
甲基苯乙烯
合成路线
（共 483 条）
873-66-5
甲基苯乙烯
→
反应条件
4518-66-5
(1S,2S)-(-)-1-苯基亚丙基环氧
+
14212-54-5
1(1R,2R)-(+)-1-苯基亚丙基环氧
反应条件
C60H42Cl5N2O3Ru; oxygen in chlorobenzene T=25°C; 24 h; optical yield given as percent eeenantioselective reaction;
参考文献
Koya, Shota; Nishioka, Yota; Mizoguchi, Hirotaka; Uchida, Tatsuya; Katsuki, Tsutomu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 33 p. 8243 - 8246
873-66-5
甲基苯乙烯
→
反应条件
14212-53-4
+
4436-22-0
2-甲基-3-苯基环氧乙烷
+
4518-66-5
(1S,2S)-(-)-1-苯基亚丙基环氧
+
14212-54-5
1(1R,2R)-(+)-1-苯基亚丙基环氧
反应条件
Oxonereg;; potassium carbonate; acetic acid; chiral 1a-methyl-3-fluoro-3-methyldecal-2-one in ethylene glycol dimethyl ether; water T=25°C; pH=8.5 - 9; 6 h; Title compound not separated from byproducts;
参考文献
Solladie-Cavallo, Arlette; Jierry, Loic; Klein, Arlette; Schmitt, Michel; Welter, Richard
Tetrahedron Asymmetry, 2004 , vol. 15, # 24 p. 3891 - 3898
873-66-5
甲基苯乙烯
+
2587-00-0
4-二甲胺基吡啶N-氧化物
→
反应条件
2402-78-0
2,6-二氯吡啶
+
4518-66-5
(1S,2S)-(-)-1-苯基亚丙基环氧
+
14212-54-5
1(1R,2R)-(+)-1-苯基亚丙基环氧
反应条件
chiral ruthenium porphyrin complex catalyst in toluene T=-10°C; 48 h; Title compound not separated from byproducts.;
参考文献
Gross, Zeev; Ini, Santiago
Organic Letters, 1999 , vol. 1, # 13 p. 2077 - 2080
873-66-5
甲基苯乙烯
+
108167-42-6
→
反应条件
4518-66-5
(1S,2S)-(-)-1-苯基亚丙基环氧
+
14212-54-5
1(1R,2R)-(+)-1-苯基亚丙基环氧
反应条件
in benzene T=25°C; 48 h; Yield given;
参考文献
Davis, Franklin A.; Chattopadhyay, Sankar
Tetrahedron Letters, 1986 , vol. 27, # 42 p. 5079 - 5082
873-66-5
甲基苯乙烯
→
反应条件
14371-10-9
桂皮醛
+
4407-36-7
3-苯基丙-2-烯-1-醇
+
4518-66-5
(1S,2S)-(-)-1-苯基亚丙基环氧
反应条件
Agrocybe aegerita peroxygenase; dihydrogen peroxide in water; acetonitrile pH=7; 0.166667 h; potassium phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Kluge, Martin; Ullrich, Rene; Scheibner, Katrin; Hofrichter, Martin
Green Chemistry, 2012 , vol. 14, # 2 p. 440 - 446
873-66-5
甲基苯乙烯
→
反应条件
反应条件
1: 3-chloro-benzenecarboperoxoic acid 2: C68H92Cr2N8O4(2+)*2Cl(1-) / methanol; dichloromethane / 18 h / 20 °C View Scheme
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
873-66-5
甲基苯乙烯
→
反应条件
1231758-02-3
反应条件
1: 3-chloro-benzenecarboperoxoic acid 2: C68H92Cr2N8O4(2+)*2Cl(1-) / methanol; dichloromethane / 30 h / 20 °C View Scheme
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
873-66-5
甲基苯乙烯
→
反应条件
1231758-03-4
反应条件
1: 3-chloro-benzenecarboperoxoic acid 2: C68H92Cr2N8O4(2+)*2Cl(1-) / methanol; dichloromethane / 24 h / 20 °C View Scheme
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
873-66-5
甲基苯乙烯
→
反应条件
1231758-04-5
反应条件
1: 3-chloro-benzenecarboperoxoic acid 2: C68H92Cr2N8O4(2+)*2Cl(1-) / methanol; dichloromethane / 20 h / 20 °C View Scheme
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
873-66-5
甲基苯乙烯
→
反应条件
4518-66-5
(1S,2S)-(-)-1-苯基亚丙基环氧
+
14212-54-5
1(1R,2R)-(+)-1-苯基亚丙基环氧
反应条件
1: 3-chloro-benzenecarboperoxoic acid 2: C68H92Cr2N8O4(2+)*2Cl(1-) / methanol; dichloromethane / 24 h / 20 °C View Scheme
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
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