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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯甲醇
合成路线
（共 450 条）
873-76-7
4-氯苯甲醇
→
反应条件
56428-00-3
+
19048-85-2
(4-氯苯基)甲基4-氯苯甲酸酯
+
104-88-1
4-氯苯甲醛
反应条件
1: thionyl chloride; pyridine / dichloromethane 2: dimethylsulfoxide-d6 / 35 °C / |Irradiation View Scheme
参考文献
Grenga, Paolo N.; Stoutenburg, Eric G.; Priefer, Ronny
Tetrahedron Letters, 2012 , vol. 53, # 37 p. 4933 - 4937
873-76-7
4-氯苯甲醇
→
反应条件
375854-57-2
反应条件
1: phosphorus tribromide / dichloromethane / 1 h / 20 °C 2: sodium azide / dimethyl sulfoxide / 16.5 h / 0 - 20 °C 3: trifluorormethanesulfonic acid / toluene / 3 h / 20 °C 4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h View Scheme
参考文献
Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Gettongsong, Tanita
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1463 - 1467
873-76-7
4-氯苯甲醇
→
反应条件
3717-24-6
(NE)-N-[(4-氯苯基)亚甲基]羟胺
反应条件
hydrogenchloride; potassium nitrate; tin(ll) chloride in ethanol; water T=20°C; 6 h; Electrochemical reaction;
参考文献
Zhang, Li; Chen, He; Zha, Zhenggen; Wang, Zhiyong
Chemical Communications, 2012 , vol. 48, # 52 p. 6574 - 6576
873-76-7
4-氯苯甲醇
→
反应条件
114081-08-2
N-苄基-3-吡啶胺
反应条件
1: palladium diacetate; cesium hydroxide monohydrate / neat (no solvent) / 24 h / 135 °C / |Sealed tube 2: palladium diacetate; sodium hydroxide / neat (no solvent) / 24 h / 135 °C / |Sealed tube View Scheme
参考文献
Yu, Xiaochun; Jiang, Lan; Li, Qiang; Xu, Qing; Xie, Yuanyuan
Chinese Journal of Chemistry, 2012 , vol. 30, # 10 p. 2322 - 2332,11
873-76-7
4-氯苯甲醇
+
88-75-5
邻硝基苯酚
→
反应条件
1141-35-1
2-(4-氯苯基)-苯并噁唑
反应条件
1,1'-bis-(diphenylphosphino)ferrocene in toluene T=150°C; 24 h; Inert atmosphere;
参考文献
Wu, Mingyue; Hu, Xiong; Liu, Juan; Liao, Yunfeng; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 11 p. 2722 - 2725
95-55-6
邻氨基苯酚
+
873-76-7
4-氯苯甲醇
→
反应条件
1141-35-1
2-(4-氯苯基)-苯并噁唑
反应条件
[RuCl(CO)(PPh3)(PNS-Me)]; potassium hydroxide in toluene T=100°C; 24 h;
参考文献
Ramachandran, Rangasamy; Prakash, Govindan; Selvamurugan, Sellappan; Viswanathamurthi, Periasamy; Malecki, Jan Grzegorz; Ramkumar, Venkatachalam
Dalton Transactions, 2014 , vol. 43, # 21 p. 7889 - 7902
108-90-7
氯苯
+
873-76-7
4-氯苯甲醇
→
反应条件
101-76-8
1,1’-亚甲基双(4-氯苯)
+
52094-02-7
反应条件
silica gel supported phosphorus pentoxide T=20°C; 0.166667 h; Neat (no solvent);
参考文献
Khazaei, Ardeshir; Rad, Mohammad Navid Soltani; Borazjani, Maryam Kiani; Moradian, Khadijeh Mansouri; Borazjani, Mohammad Kiani; Zebarjadian, Mohammad Hassan
South African Journal of Chemistry, 2011 , vol. 64, p. 120 - 126
70-55-3
+
873-76-7
4-氯苯甲醇
→
反应条件
10504-98-0
反应条件
Wilkinson's catalyst; potassium carbonate T=120°C; 12 h; Sealed tube;
参考文献
Feng, Sun Lin; Liu, Chuan Zhi; Li, Qiang; Yu, Xiao Chun; Xu, Qing
Chinese Chemical Letters, 2011 , vol. 22, # 9 p. 1021 - 1024
873-76-7
4-氯苯甲醇
→
反应条件
10504-98-0
反应条件
1: acetic acid; hydrogen bromide / 0.5 h / 0 °C 2: ammonia / ethanol; water / 4 h / 20 °C 3: triethylamine / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Kiruthika, Selvarangam E.; Perumal, Paramasivan Thirumalai
Organic Letters, 2014 , vol. 16, # 2 p. 484 - 487
70-55-3
+
873-76-7
4-氯苯甲醇
→
反应条件
反应条件
silver trifluoromethanesulfonate in nitromethane T=100°C; 8 h; Product distribution; Further Variations:SolventsCatalysts;
参考文献
Sreedhar; Surendra Reddy; Amarnath Reddy; Neelima; Arundhathi
Tetrahedron Letters, 2007 , vol. 48, # 46 p. 8174 - 8177
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