3,3,5-三甲基环己酮合成路线 （共 69 条）
反应条件
hydrogen; palladium 10 on activated carbon T=220°C; P=749.884 Torr; 6 h; Product distribution / selectivity;
参考文献
WO2009/85826 A2, ;
Page/Page column 8 ;
反应条件
lithium perchlorate; triethylamine in acetonitrile 3 h; Irradiation;
参考文献
Cossy, Janine; Furet, Nathalie; BouzBouz, Samir
Tetrahedron, 1995 , vol. 51, # 43 p. 11751 - 11764
反应条件
1: methyl-magnesium iodide With copper(l) chloride in diethyl ether complexation; 0.0833333 h; cooling; 2: 3,5-dimethyl-cyclohex-2-en-1-one in diethyl ether Addition; 1 h; cooling;
参考文献
Jirgensons, Aigars; Kauss, Valerjans; Kalvinsh, Ivars; Gold, Markus R.; Danysz, Wojciech; Parsons, Chris G.; Quack, Gunter
European Journal of Medicinal Chemistry, 2000 , vol. 35, # 6 p. 555 - 565
反应条件
2,5-dimethyl-2,5-dihydroxy hexane; nickel diacetate; sodium hydride; magnesium bromide in tetrahydrofuran T=63°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 29, # 12 p. 1383 - 1384
反应条件
Li(1+)*C12H28AlO3(1-) in tetrahydrofuran; hexane T=-78°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 49, # 10 p. 1717 - 1724
反应条件
tetra-N-butylammonium borohydride in toluene T=95°C; 20 h; Yield given;
参考文献
D'Incan, E.; Loupy, A.
Tetrahedron, 1981 , vol. 37, p. 1171 - 1180
反应条件
water; pyridinium p-toluenesulfonate; acetone
参考文献
Journal of the American Chemical Society, , vol. 131, # 40 p. 14584 - 14589
反应条件
sulfuric acid; water; dihydrogen peroxide in tetrahydrofuran T=20 - 25°C; 24 h;
参考文献
Russian Journal of General Chemistry, , vol. 80, # 8 p. 1667 - 1671
反应条件
carbon dioxide; hydrogen T=350°C; P=90009 Torr; Supercritical conditionsFlow reactor;
参考文献
Organic Process Research and Development, , vol. 2, # 3 p. 137 - 146
反应条件
Co(1,2-bis-(diphenylphosphino)ethane)Cl2 in diethyl ether T=-40°C; 1 h;
参考文献
Chemische Berichte, , vol. 119, # 5 p. 1581 - 1593
