3,3,5-三甲基环己酮合成路线 (共 69 条)
反应条件
5-palladium/activated carbon T=150°C; 4 h; Product distribution / selectivity;
参考文献
WO2009/85826 A2, ;
Page/Page column 7 ;
反应条件
hydrogen T=20°C; P=750.075 Torr; 0.5 h; Reagent/catalystTime;
参考文献
Dalton Transactions, , vol. 41, # 41 p. 12666 - 12669
反应条件
triethylamine in methanol Irradiation;
参考文献
Tetrahedron Letters, , vol. 31, # 47 p. 6793 - 6796
反应条件
methyllithium; dimethyl zinc; Co(acetylacetonate)3 1.) ether, 0 deg C, 15 min, 2.) -40 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 119, # 5 p. 1581 - 1593
反应条件
carbon dioxide; hydrogen; 5 Pd on alumina T=50°C; 0.166667 - 1 h; Product distribution / selectivity;
参考文献
JP2005/112774 A, ;
Page/Page column 8-10 ;
反应条件
potassium hydroxide anschl. Dehydrieren an ZnO;
参考文献
US2692289 , ;
DRP/DRBP Org.Chem.
DE840695 , ;
反应条件
phenylphosphoric acid dichloride; N,N-dimethyl-formamide; sodium iodide 1.) acetonitrile, few min, room temp., 2.) 5 h, room temp.; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 29, # 43 p. 5471 - 5474
反应条件
sodium hydroxide; sodium tetrahydroborate in water T=14.9°C; with and without var. hydrotropes; other temp.; Product distribution;
参考文献
Synthetic Communications, , vol. 20, # 1 p. 111 - 117
反应条件
triethylamine in acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 34, # 50 p. 8107 - 8110
Tetrahedron, , vol. 51, # 43 p. 11751 - 11764
反应条件
T=25°C; Equilibrium constant;
参考文献
Canadian Journal of Chemistry, , vol. 36, p. 656