反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1964227', constants.ctx, '0')">1,4-DITFB</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78°C; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1900390', constants.ctx, '0')">carbon dioxide</a> T=-78 - 0°C; Large scale reaction; <br />
参考文献
Aakeroey, Christer B.; Chopade, Prashant D.; Ganser, Claudia; Desper, John Chemical Communications, 2011 , vol. 47, # 16 p. 4688 - 4690