R-(3)-苄氧基肉豆蔻酸合成路线 （共 14 条）
反应条件
1: CF3SO3H / cyclohexane; CH2Cl2 / 0.5 h / Ambient temperature
2: TFA / CH2Cl2 / 22 h / Ambient temperature
View Scheme
参考文献
Oikawa, Masato; Kusumoto, Shoichi
Tetrahedron: Asymmetry, 1995 , vol. 6, # 4 p. 961 - 966
反应条件
1: 75 percent / NaOMe / methanol / 3 h / 0 °C
2: CF3SO3H / cyclohexane; CH2Cl2 / 0.5 h / Ambient temperature
3: TFA / CH2Cl2 / 22 h / Ambient temperature
View Scheme
参考文献
Oikawa, Masato; Kusumoto, Shoichi
Tetrahedron: Asymmetry, 1995 , vol. 6, # 4 p. 961 - 966
反应条件
1: 99 percent / Bu3SnH, AIBN / benzene / 6 h / Heating
2: 75 percent / NaOMe / methanol / 3 h / 0 °C
3: CF3SO3H / cyclohexane; CH2Cl2 / 0.5 h / Ambient temperature
4: TFA / CH2Cl2 / 22 h / Ambient temperature
View Scheme
参考文献
Oikawa, Masato; Kusumoto, Shoichi
Tetrahedron: Asymmetry, 1995 , vol. 6, # 4 p. 961 - 966
反应条件
1: 74 percent / trifluoromethanesulfonic acid / CH2Cl2 / 2 h / 0 °C
2: 80 percent / zinc dust / acetic acid / 3 h / 50 °C
View Scheme
参考文献
Imoto, Masahiro; Yoshimura, Hiroyuki; Yamamoto, Michiharu; Shimamoto, Tetsuo; Kusumoto, Shoichi; Shiba, Tetsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 2197 - 2204
