反应条件
1.1: sec.-butyllithium; N,N,N',N,-tetramethylethylenediamine / cyclohexane / 0.75 h / -78 °C
1.2: 0.75 h / -78 °C
2.1: cyclohexane; toluene / 0.75 h / -78 °C
3.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 1 h / 20 °C
3.2: 3 h / 95 °C
View Scheme
参考文献
Gross, Timothy D.; Chou, Shine; Bonneville, Daniel; Gross, Raymond S.; Wang, Peng; Campopiano, Onorato; Ouellette, Michael A.; Zook, Scott E.; Reddy, Jayachandra P.; Moree, Wilna J.; Jovic, Florence; Chopade, Shubham
Organic Process Research and Development, 2008 , vol. 12, # 5 p. 929 - 939
