1.1: triethylamine / dichloromethane / 0 - 20 °C 1.2: 0.25 h / 20 °C 2.1: didodecanoyl peroxide / 1,2-dichloro-ethane / 4 h / Reflux 3.1: trifluorormethanesulfonic acid / 24 h / Reflux View Scheme

ZnCp*2; hydrogen; C{N(2,6-iPr2C6H3)CH}2 in benzene-d6 T=50°C; P=75007.5 Torr; 72 h; Inert atmosphere; Reagent/catalystTemperatureTimePressure;