反应条件
1: N1,N3-Dimethyluracil With 2,6-di-tert-butyl-pyridine; bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran
T=80°C; 24 h; Sealed tubeInert atmosphere;
2: Togni’s reagent With 1,10-phenanthroline; copper(I) thiophene-2-carboxylate; lithium hydroxide hydrate in tetrahydrofuran; dichloromethane
T=50°C; 22 h; Reflux;
参考文献
Cernova, Miroslava; Pohl, Radek; Klepetarova, Blanka; Hocek, Michal
Heterocycles, 2014 , vol. 89, # 5 p. 1159 - 1171
