2-(2-硝基乙烯基)噻吩合成路线 （共 10 条）
反应条件
ammonium acetate T=90°C; Henry reaction; 1 h; Microwave irradiation;
参考文献
Rodriguez, Jose M.; Dolors Pujol
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2629 - 2632
反应条件
ammonium acetate T=90°C; Henry reaction; 0.416667 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 52, # 21 p. 2629 - 2632
反应条件
H-Y (SiO2/Al2O3 = 5.6) zeolite T=60°C; Aza-Henry reaction; 9 h;
参考文献
Applied Catalysis A: General, , vol. 388, # 1-2 p. 211 - 215
反应条件
NSC26899 in acetonitrile T=80°C;
参考文献
Tintillier, P.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Tetrahedron Letters, 1986 , vol. 27, # 21 p. 2357 - 2360
反应条件
formic acid; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; triethylamine; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide in ethyl acetate T=28°C; 3 h; chemoselective reaction;
参考文献
Xiang, Jing; Sun, Er-Xiao; Lian, Chun-Xia; Yuan, Wei-Cheng; Zhu, Jin; Wang, Qiwei; Deng, Jingen
Tetrahedron, 2012 , vol. 68, # 24 p. 4609 - 4620
反应条件
NSC26899 in acetonitrile T=80°C;
参考文献
Tintillier, P.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Tetrahedron Letters, 1986 , vol. 27, # 21 p. 2357 - 2360
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Meth-Cohn, Otto; Vij, Rup Rani; Smalley, Robert K.; Bass, Robert J.
Journal of Chemical Research, Miniprint, 1989 , # 5 p. 1001 - 1018
反应条件
in toluene 1 h; RefluxDry air;
参考文献
Chu, Cheng-Ming; Tu, Zhijay; Wu, Pohsi; Wang, Chieh-Chieh; Liu, Ju-Tsung; Kuo, Chun-Wei; Shin, Yu-Hsuan; Yao, Ching-Fa
Tetrahedron, 2009 , vol. 65, # 19 p. 3878 - 3885
反应条件
[BmIm]OH; air in ethanol
4 h; Reflux;
参考文献
Babu, G. Neelaiah; Ayalew, Haile Micheal; Jain, Shubha
Medicinal Chemistry Research, 2014 , vol. 23, # 5 p. 2608 - 2614
反应条件
1: HCO2H / 0.67 h / 80 °C
2: LiAlH4 / diethyl ether / Heating
View Scheme
参考文献
Styngach,E.P. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1973 , vol. 9, p. 1378 - 1382
Khimiya Geterotsiklicheskikh Soedinenii, 1973 , vol. 9, # 11 p. 1523 - 1527
