反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; silver perchlorate; calcium carbonate
1.) nitromethane, -15 deg C, 2.) benzene, reflux, 4.5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Halazy, Serge; Hevesi, Laszlo
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5242 - 5246