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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87411-43-6
合成路线
（共 7 条）
1111235-07-4
→
反应条件
87411-43-6
反应条件
sodium hydroxide in tetrahydrofuran; water 2 h; Reflux;
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
5454-83-1
5-溴戊酸甲酯
→
反应条件
87411-43-6
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C 2: sodium hydroxide / water; tetrahydrofuran / 2 h / |Reflux View Scheme
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
2067-33-6
5-溴戊酸
→
反应条件
87411-43-6
反应条件
1: thionyl chloride / 2 h / 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C 3: sodium hydroxide / water; tetrahydrofuran / 2 h / |Reflux View Scheme
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
554-84-7
间硝基苯酚
→
反应条件
87411-43-6
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C 2: sodium hydroxide / water; tetrahydrofuran / 2 h / |Reflux View Scheme
参考文献
Zhang, Xuan; Bao, Bin; Yu, Xiuhua; Tong, Linjiang; Luo, Yu; Huang, Qingqing; Su, Mingbo; Sheng, Li; Li, Jia; Zhu, Hong; Yang, Bo; Zhang, Xiongwen; Chen, Yi; Lu, Wei
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 22 p. 6981 - 6995
104295-63-8
→
反应条件
87411-43-6
反应条件
hydrogenchloride; acetic acid
参考文献
Gerecs; Windholz
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 14, p. 417,418
6280-87-1
5-氯戊腈
→
反应条件
87411-43-6
反应条件
1: tetrahydrofurfuryl alcohol 2: acetic acid; aqueous hydrochloric acid View Scheme
参考文献
Gerecs; Windholz
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 14, p. 417,418
3019-85-0
→
反应条件
87411-43-6
反应条件
1: tetrahydrofurfuryl alcohol 2: acetic acid; aqueous hydrochloric acid View Scheme
参考文献
Gerecs; Windholz
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 14, p. 417,418
