1: tetraethylene glycol With sodium hydride in tetrahydrofuran; mineral oil
1 h;
2: 3-(chloro)-prop-1-yne in tetrahydrofuran; mineral oil
T=20°C; 20 h; Cooling with ice;
参考文献
Sung, Sae Reum; Han, Seung Choul; Jin, Sung-Ho; Lee, Jae Wook
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 11 p. 3933 - 3940