2,3-二甲基咪唑并[1,2-a]吡啶合成路线 (共 3 条)
反应条件
potassium hydroxide in 1,4-dioxane
T=200 - 210°C; P=12160 Torr; 1 h;
参考文献
Andriyankov, M. A.; Belobrysova, O. V.; Chipanina, N. N.; Afonin, A. V.; Kukharev, B. F.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 12 p. 2519 - 2521
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 12 p. 2747 - 2750
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in tetrahydrofuran
T=210°C; 12 h;
参考文献
Kondo, Teruyuki; Kotachi, Shinji; Ogino, Shin-ichi; Watanabe, Yoshihisa
Chemistry Letters, 1993 , # 8 p. 1317 - 1320
反应条件
RuCl2(PPh3)2 in diethylene glycol dimethyl ether
24 h; Heatingother vincinal-diols, acetoin, and 5-substituted-2-aminopyridines; Mechanism;
参考文献
Kondo, Teruyuki; Kotachi, Shinji; Ogino, Shin-ichi; Watanabe, Yoshihisa
Chemistry Letters, 1993 , # 8 p. 1317 - 1320