反应条件
1.1: 92 percent / diisobutylaluminium hydride / toluene / 0.33 h / -78 °C
2.1: 66 percent / N-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH2Cl2 / 1.5 h / 0 °C
3.1: n-BuLi / tetrahydrofuran; toluene / 0.17 h / 0 °C
3.2: 90 percent / tetrahydrofuran; toluene / 1 h / -20 °C
View Scheme
参考文献
Ishii, Yusuke; Nagumo, Shinji; Arai, Takayuki; Akuzawa, Masami; Kawahara, Norio; Akita, Hiroyuki
Tetrahedron, 2006 , vol. 62, # 4 p. 716 - 725
