反应条件
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; toluene
T=0°C; 0.166667 h;
2: (4S,5R,6R)-5,7-isopropylidenedioxy-4,6-dimethyl-heptanal in tetrahydrofuran; toluene
T=-20°C; Wittig homologation; 1 h;
参考文献
Ishii, Yusuke; Nagumo, Shinji; Arai, Takayuki; Akuzawa, Masami; Kawahara, Norio; Akita, Hiroyuki
Tetrahedron, 2006 , vol. 62, # 4 p. 716 - 725
