1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 h / 75 °C 2: N-iodo-succinimide / acetone / 4 h / 20 °C View Scheme
参考文献
UNIVERSITY OF ROCHESTER; BOARD OF REGENTS OF THE UNIVERSITY OF NEBRASKA; GELBARD, Harris A.; DEWHURST, Stephen; GENDELMAN, Howard E.
Patent: WO2014/85795 A1, 2014 ;
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 h / 75 °C
2.1: N-iodo-succinimide / acetone / 4 h / 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
3.2: 3 h / 20 °C
View Scheme
参考文献
UNIVERSITY OF ROCHESTER; BOARD OF REGENTS OF THE UNIVERSITY OF NEBRASKA; GELBARD, Harris A.; DEWHURST, Stephen; GENDELMAN, Howard E.
Patent: WO2014/85795 A1, 2014 ;
