(5Z)-2-(4-氯苯基)-5-(3H-吲哚-3-亚基)-3-苯基-2,5-二氢-1H-四唑-3-鎓碘化物合成路线 （共 4 条）
反应条件
sulfuric acid; dihydrogen peroxide; iron(II) sulfate in ethanol
T=100°C; 2 h;
参考文献
Sathi; Gujrati; Nath; Agarwal; Bhargava; Shanker
Arzneimittel-Forschung/Drug Research, 1983 , vol. 33, # 9 p. 1218 - 1221
反应条件
1: glacial AcOH / ethanol / 4 h / Heating
2: 1.) conc.HCl, NaNO2 / 1.) glacial AcOH, H2O, 0 - 5 deg C, 2.) pyridine, below 10 deg C - room temp.
3: 40 percent / 2 N H2SO4, 20percent H2O2, FeSO4 / ethanol / 2 h / 100 °C
View Scheme
参考文献
Sathi; Gujrati; Nath; Agarwal; Bhargava; Shanker
Arzneimittel-Forschung/Drug Research, 1983 , vol. 33, # 9 p. 1218 - 1221
反应条件
1: 1.) conc.HCl, NaNO2 / 1.) glacial AcOH, H2O, 0 - 5 deg C, 2.) pyridine, below 10 deg C - room temp.
2: 40 percent / 2 N H2SO4, 20percent H2O2, FeSO4 / ethanol / 2 h / 100 °C
View Scheme
参考文献
Sathi; Gujrati; Nath; Agarwal; Bhargava; Shanker
Arzneimittel-Forschung/Drug Research, 1983 , vol. 33, # 9 p. 1218 - 1221
反应条件
1: glacial AcOH / ethanol / 4 h / Heating
2: 1.) conc.HCl, NaNO2 / 1.) glacial AcOH, H2O, 0 - 5 deg C, 2.) pyridine, below 10 deg C - room temp.
3: 40 percent / 2 N H2SO4, 20percent H2O2, FeSO4 / ethanol / 2 h / 100 °C
View Scheme
参考文献
Sathi; Gujrati; Nath; Agarwal; Bhargava; Shanker
Arzneimittel-Forschung/Drug Research, 1983 , vol. 33, # 9 p. 1218 - 1221
