2-[2-[1-(1-硫代羧基六氢-1H-氮杂卓-2-基)肼基]乙基]吡啶1-氧化物合成路线 (共 3 条)
反应条件
in ethanol
4 h; Heating;
参考文献
Scovill, John P.; Klayman, Daniel L.; Lambros, Chris; Childs, George E.; Notsch, John D.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 1 p. 87 - 91
反应条件
1: 78 percent / methanol / 0.5 h / 50 °C
2: 92 percent / NaBH4 / ethanol / 1 h / Ambient temperature
3: 58 percent / ethanol / 4 h / Heating
View Scheme
参考文献
Scovill, John P.; Klayman, Daniel L.; Lambros, Chris; Childs, George E.; Notsch, John D.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 1 p. 87 - 91
反应条件
1: 92 percent / NaBH4 / ethanol / 1 h / Ambient temperature
2: 58 percent / ethanol / 4 h / Heating
View Scheme
参考文献
Scovill, John P.; Klayman, Daniel L.; Lambros, Chris; Childs, George E.; Notsch, John D.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 1 p. 87 - 91