2-氨基-5-甲基三氟甲基苯合成路线 （共 4 条）
反应条件
2-picoline; Na2S2O5; sulfur dioxide; zinc in N,N-dimethyl-formamide T=20°C; P=2250.2 - 3750.3 Torr; 2 h;
参考文献
Wakselman, Claude; Tordeux, Marc
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1701 - 1703
反应条件
hydrogenchloride; iron in 1,4-dioxane; water
参考文献
Rhone-Poulenc Specialites Chimiques
Patent: US4731450 A1, 1988 ;
反应条件
sodium sulfide; nitric acid; ammonium chloride; sulfur 1.) 15 min, 2.) methanol, H2O, 75 deg C, 5 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 51, # 20 p. 3903 - 3904
