3-溴-1-(三异丙基硅基)吡咯合成路线 （共 23 条）
反应条件
n-butyllithium 1.) THF, hexane, -23 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Kozikowski, Alan P.; Cheng, Xue-Min
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3239 - 3240
反应条件
n-butyllithium 1.) THF, hexane, -23 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Kozikowski, Alan P.; Cheng, Xue-Min
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3239 - 3240
反应条件
n-butyllithium; N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide 1.) THF, hexane, -78 deg C, 0.5 h, 2.) THF, hexane, a) -78 deg C, 0.5 h, b) RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Barnes; Hu; Hunt
Synthetic Communications, 1994 , vol. 24, # 12 p. 1749 - 1755
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78°C; 2: With boric acid trimethyl ester 3: With methanol Further stages.;
参考文献
Nadeau, Jocelyn M.; Swager, Timothy M.
Tetrahedron, 2004 , vol. 60, # 34 p. 7141 - 7146
反应条件
1: 3-bromo-1-(triisopropylsilyl)pyrrole With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; Inert atmosphere; 2: boric acid trimethyl ester in tetrahydrofuran T=-78 - 20°C; 1 h; 3: With water in tetrahydrofuran
参考文献
Takase, Masayoshi; Inabe, Ayumi; Sugawara, Yuki; Fujita, Wataru; Nishinaga, Tohru; Nomura, Kotohiro
Organic Letters, 2013 , vol. 15, # 13 p. 3202 - 3205
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 1.5 h; Heating;
参考文献
Bumagin, N. A.; Nikitina, A. F.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 10 p. 1619 - 1629
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 10 p. 1537 - 1547
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 1.5 h; Heating;
参考文献
Bumagin, N. A.; Sokolova, A. F.; Beletskaya, I. P.; Wolz, G.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.2 p. 136 - 137
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 162 - 164
反应条件
1: magnesium / tetrahydrofuran / 3 h / Heating 2: 80 percent / PdCl2(1,1'-bis(diphenylphosphino)ferrocene) / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Bumagin, N. A.; Nikitina, A. F.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 10 p. 1619 - 1629
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 10 p. 1537 - 1547
参考文献
Stefan, Klaus-Peter; Schuhmann, Wolfgang; Parlar, Harun; Korte, Friedhelm
Chemische Berichte, 1989 , vol. 122, p. 169 - 174
反应条件
n-butyllithium
1.) THF, hexane, -23 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Kozikowski, Alan P.; Cheng, Xue-Min
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3239 - 3240
