反应条件
titanium(IV) isopropylate; iso-propylmagnesium bromide
1.) ether, -78 deg C -> -50 deg C, 1 h, - 50 deg C, 2 h; 2.) -78 deg C, 30 min, -78 deg C -> 0 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Yamashita, Koki; Sato, Fumie
Tetrahedron Letters, 1996 , vol. 37, # 40 p. 7275 - 7278