反应条件
1: 18 percent / 7.5 N aq.HCl / ethanol / 0.17 h / Heating
2: 40 percent / LiAlH4 / diethyl ether / 3 h / Heating
3: 2 h / 180 °C
4: 1.) POCl3, 2.) NaBH4 / 1.) toluene, reflux, 1 h; 2.) MeOH, room temp.
View Scheme
参考文献
Knefeli, Frank; Mayer, Klaus K.; Poettinger, Theodor; Stoeber, Georg; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1983 , vol. 316, # 9 p. 773 - 781
