3,4-二甲氧苄基异氰酸酯合成路线 （共 4 条）
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran
T=-80°C;
参考文献
Hirota, Kosaku; Kazaoka, Kazunori; Niimoto, Itaru; Sajiki, Hironao
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 8 p. 1354 - 1365
反应条件
1: SOCl2; DMF / 5 h / 0 °C
2: NaN3 / acetone; H2O / 4 h / 0 °C
3: benzene / 5 h / Heating
View Scheme
参考文献
Park, See-Hyoung; Kang, Sun-Hee; Lim, Sang-Hyeong; Oh, Hyun-Sik; Lee, Keun-Hyeung
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 20 p. 3455 - 3459
反应条件
1: NaN3 / acetone; H2O / 4 h / 0 °C
2: benzene / 5 h / Heating
View Scheme
参考文献
Park, See-Hyoung; Kang, Sun-Hee; Lim, Sang-Hyeong; Oh, Hyun-Sik; Lee, Keun-Hyeung
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 20 p. 3455 - 3459
反应条件
in benzene
Curtius rearrangement; 5 h; Heating;
参考文献
Park, See-Hyoung; Kang, Sun-Hee; Lim, Sang-Hyeong; Oh, Hyun-Sik; Lee, Keun-Hyeung
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 20 p. 3455 - 3459
