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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87687-37-4
合成路线
（共 9 条）
→
反应条件
87687-37-4
反应条件
triphenylphosphine; Bu4N[Fe(CO)3(NO)] in N,N-dimethyl-formamide T=80°C; 12 h; Title compound not separated from byproducts;
参考文献
Plietker, Bernd
Angewandte Chemie - International Edition, 2006 , vol. 45, # 9 p. 1469 - 1473
87687-35-2
→
反应条件
87687-37-4
反应条件
water; zinc in acetic acid Ambient temperature;
参考文献
Kolsaker, Per; Storesund, Hans-Johan; Gulbrandsen, Trygve; Woien, Grete
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 3 p. 187 - 196
24509-88-4
1,1-二甲基-2-丙烯基乙酸酯
+
109-77-3
丙二腈
→
反应条件
87687-37-4
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran 36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
109-77-3
丙二腈
+
164513-96-6
→
反应条件
87687-37-4
反应条件
triphenylphosphine; Bu4N[Fe(CO)3(NO)] in N,N-dimethyl-formamide 24 h; Product distribution / selectivity;
参考文献
Plietker, Bernd
Patent: US2007/49770 A1, 2007 ;
Location in patent: Page/Page column 3; Sheet 3 ;
109-77-3
丙二腈
→
反应条件
87687-37-4
反应条件
tetrabutylammomium bromide
参考文献
Benati, Luisa; Bencivenni, Giorgio; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Scialpi, Rosanna; Spagnolo, Piero; Zanardi, Giuseppe; Rizzoli, Corrado
Organic Letters, 2004 , vol. 6, # 3 p. 417 - 420
87687-37-4
+
106-93-4
二溴乙烷
→
反应条件
649759-64-8
反应条件
potassium tert-butylate; tetrabutylammomium bromide
参考文献
Benati, Luisa; Bencivenni, Giorgio; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Scialpi, Rosanna; Spagnolo, Piero; Zanardi, Giuseppe; Rizzoli, Corrado
Organic Letters, 2004 , vol. 6, # 3 p. 417 - 420
87687-37-4
+
109-64-8
→
反应条件
649759-69-3
反应条件
potassium tert-butylate; tetrabutylammomium bromide
参考文献
Benati, Luisa; Bencivenni, Giorgio; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Scialpi, Rosanna; Spagnolo, Piero; Zanardi, Giuseppe; Rizzoli, Corrado
Organic Letters, 2004 , vol. 6, # 3 p. 417 - 420
87687-37-4
→
反应条件
649759-78-4
反应条件
1: 41 percent / tetrabutylammonium bromide; potassium tert-butoxide 2: 90 percent / sodium azide / dimethylsulfoxide View Scheme
参考文献
Benati, Luisa; Bencivenni, Giorgio; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Scialpi, Rosanna; Spagnolo, Piero; Zanardi, Giuseppe; Rizzoli, Corrado
Organic Letters, 2004 , vol. 6, # 3 p. 417 - 420
87687-37-4
→
反应条件
649759-84-2
反应条件
1: 75 percent / tetrabutylammonium bromide; potassium tert-butoxide 2: 86 percent / sodium azide / dimethylsulfoxide View Scheme
参考文献
Benati, Luisa; Bencivenni, Giorgio; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Scialpi, Rosanna; Spagnolo, Piero; Zanardi, Giuseppe; Rizzoli, Corrado
Organic Letters, 2004 , vol. 6, # 3 p. 417 - 420
