1: 80 percent / K-Selectride / tetrahydrofuran / 5 h / -50 - -45 °C 2: hydrofluoric acid / acetonitrile / 1 h / -5 °C 3: base hydrolysis View Scheme
参考文献
Cai, Zuyun; Nassium, Bahman; Crabbe, Pierre
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 7 p. 1573 - 1578
1: 80 percent / K-Selectride / tetrahydrofuran / 5 h / -50 - -45 °C 2: hydrofluoric acid / acetonitrile / 1 h / -5 °C View Scheme
参考文献
Cai, Zuyun; Nassium, Bahman; Crabbe, Pierre
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 7 p. 1573 - 1578
1: 83 percent / morphilinosulfotrifluoride / CH2Cl2 / 1 h / -78 °C 2: 75 percent / aq. acetic acid, 1N HCl / tetrahydrofuran / 30 h / 25 °C 3: alkaline medium View Scheme
参考文献
Bezuglov, V. V.; Serkov, I. V.; Gafurov, R. G.; Bergel'son, L. D.
Doklady Chemistry, 1984 , vol. 277, p. 264 - 266
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 277, # 6 p. 1400 - 1402
