2-溴-1-苯基-1-丁酮合成路线 （共 21 条）
反应条件
N,N,N',N,-tetramethylethylenediamine; diisobutylaluminium hydride; tin(ll) chloride in tetrahydrofuran; toluene T=-78°C; 0.166667 h;
参考文献
Oriyama, Takeshi; Mukaiyama, Teruaki
Chemistry Letters, 1984 , p. 2069 - 2070
反应条件
10-methyl-9,10-dihydroacridine; perchloric acid in acetonitrile T=61.9°C; Product distributionMechanism;
参考文献
Fukuzumi, Shunichi; Mochizuki, Seiji; Tanaka, Toshio
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1497 - 1499
反应条件
perchloric acid; 10-methyl-9,10-dihydroacridine in acetonitrile-D3 T=61.9°C; 100 h; Title compound not separated from byproducts;
参考文献
Mochizuki; Fukuzumi; Tanaka
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 3049 - 3051
反应条件
lanthanum(III) bromide; lithium perchlorate in tetrahydrofuran electrolysis;
参考文献
Fry, Albert J.; Susla, Marko; Weltz, Michael
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2496 - 2498
参考文献
v. Auwers; Laemmerhirt
Chemische Berichte, 1920 , vol. 53, p. 441
反应条件
N,N-dimethyl-formamide
参考文献
Gompper; Christmann
Chemische Berichte, 1959 , vol. 92, p. 1944,1948
反应条件
N,N-dimethyl-formamide
参考文献
Gompper; Christmann
Chemische Berichte, 1959 , vol. 92, p. 1944,1948
反应条件
bromine
T=20°C; 0.333333 h;
参考文献
Lagoja, Irene M.; Pannecouque, Christophe; Van Aerschot, Arthur; Witvrouw, Myriam; Debyser, Zeger; Balzarini, Jan; Herdewijn, Piet; De Clercq, Erik
Journal of Medicinal Chemistry, 2003 , vol. 46, # 8 p. 1546 - 1553
反应条件
Oxonereg;; potassium bromide in dichloromethane; water
T=20°C; 24 h; visible light irradiation;
参考文献
Moriyama, Katsuhiko; Takemura, Misato; Togo, Hideo
Organic Letters, 2012 , vol. 14, # 9 p. 2414 - 2417
反应条件
1.1: Mg; I2 / diethyl ether
1.2: 100 percent / diethyl ether / 6 h / Heating
2.1: 100 percent / Br2 / 0.33 h / 20 °C
View Scheme
参考文献
Lagoja, Irene M.; Pannecouque, Christophe; Van Aerschot, Arthur; Witvrouw, Myriam; Debyser, Zeger; Balzarini, Jan; Herdewijn, Piet; De Clercq, Erik
Journal of Medicinal Chemistry, 2003 , vol. 46, # 8 p. 1546 - 1553
