2-溴-1-苯基-1-丁酮合成路线 （共 21 条）
反应条件
vanadium(III) chloride
1.) dichloromethane, -78 grad C, 20 min, 2.) dichloromethane, -78 grad C, 1.5 h, room temp. 16 h; Yield given. Multistep reaction;
参考文献
Hirao, Toshikazu; Misu, Daisuke; Yao, Koichi; Agawa, Toshio
Tetrahedron Letters, 1986 , vol. 27, # 8 p. 929 - 932
反应条件
aluminium trichloride
参考文献
Collet
Bulletin de la Societe Chimique de France, 1896 , vol. <3> 15, p. 1100
Bulletin de la Societe Chimique de France, 1897 , vol. <3> 17, p. 76
反应条件
carbon disulfide; aluminium trichloride
参考文献
v. Auwers; Laemmerhirt
Chemische Berichte, 1920 , vol. 53, p. 441
反应条件
1: acetonitrile; AgNO3
2: piperidine; diethyl ether
View Scheme
参考文献
Emmons; Freeman
Journal of the American Chemical Society, 1955 , vol. 77, p. 4415
反应条件
perchloric acid; 10-methyl-9,10-dihydroacridine in acetonitrile-D3
T=61.9°C; 100 h; Title compound not separated from byproducts;
参考文献
Mochizuki; Fukuzumi; Tanaka
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 3049 - 3051
反应条件
propionic acid sodium salt; propionic acid
anschliessend Erhitzen mit Ammoniumpropionat;
参考文献
Theilig
Chemische Berichte, 1953 , vol. 86, p. 96,107
反应条件
sodium ethanolate in ethanol
T=-25°C;
参考文献
Bulka,E.; Pfeiffer,W.D.
Journal fuer Praktische Chemie (Leipzig), 1976 , vol. 318, p. 971 - 982
反应条件
sodium ethanolate in ethanol
T=-25°C;
参考文献
Bulka,E.; Pfeiffer,W.D.
Journal fuer Praktische Chemie (Leipzig), 1976 , vol. 318, p. 971 - 982
反应条件
1: NaOEt / ethanol / -25 °C
2: ethanol / Heating; (dehydration)
View Scheme
参考文献
Bulka,E.; Pfeiffer,W.D.
Journal fuer Praktische Chemie (Leipzig), 1976 , vol. 318, p. 971 - 982
反应条件
1: NaOEt / ethanol / -25 °C
2: CHCl3 / Heating; (dehydration)
View Scheme
参考文献
Bulka,E.; Pfeiffer,W.D.
Journal fuer Praktische Chemie (Leipzig), 1976 , vol. 318, p. 971 - 982
