4-(三甲基甲硅烷基)苯甲醚合成路线 （共 34 条）
反应条件
NiCl2((PPh3)P)2 in 1,4-dioxane 1 h; Heating;
参考文献
Trost, Barry M.; Yoshida, Jun-ichi
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 4895 - 4898
反应条件
tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide Ambient temperatureelectrochemical reduction;
参考文献
Yoshida, Jun-Ichi; Muraki, Katsuhiko; Funanashi, Hirokatsu; Kawabata, Nariyoshi
Journal of Organometallic Chemistry, 1985 , vol. 284, p. C33 - C35
反应条件
1: 1-(2,2-dibromocyclopropyl)benzene With Me4ZnLi2 in tetrahydrofuran T=0°C; 2 h; 2: chloro-trimethyl-silane T=20°C; 2 h; Further stages.;
参考文献
Takada; Sakurai; Hirao
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 300 - 302
反应条件
bis(cyclopentadienyl)titanium dichloride; manganese in tetrahydrofuran 0.5 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 8 p. 4171 - 4176
反应条件
1: 1-bromo-4-methoxy-benzene With tetrahydrofuran; n-butyllithium in diethyl ether; cyclohexane T=20°C; Inert atmosphere; 2: chloro-trimethyl-silane in diethyl ether; cyclohexane T=20°C; 0.5 h;
参考文献
Synthesis (Germany), , vol. 44, # 16 p. 2531 - 2536
参考文献
Journal of the American Chemical Society, , vol. 95, # 16 p. 5288 - 5298
Journal of the Chemical Society, , p. 3148,3149
反应条件
1: tetrahydrofuran; para-iodoanisole With n-butyllithium in cyclohexane T=2°C; Inert atmosphere; 2: chloro-trimethyl-silane in cyclohexane T=2°C;
参考文献
Synthesis (Germany), , vol. 44, # 16 p. 2531 - 2536
反应条件
1: 1-bromo-4-methoxy-benzene With tetrahydrofuran; n-butyllithium in diethyl ether; cyclohexane T=20°C; Inert atmosphere; 2: chloro-trimethyl-silane in diethyl ether; cyclohexane T=20°C; 0.5 h;
参考文献
Synthesis (Germany), , vol. 44, # 16 p. 2531 - 2536
反应条件
n-butyllithium in tetrahydrofuran; cyclohexane T=20°C; Inert atmosphere;
参考文献
Synthesis (Germany), , vol. 44, # 16 p. 2531 - 2536
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene byproducts: Bu3SnBr, Me3SiBr; at 115°C for 15 h in sealed thick wall Pyrex glass ampoules;
参考文献
Journal of Organometallic Chemistry, , vol. 215, # 1 p. 49 - 58
