1a,7b-二氢环氧乙烷并[f]喹啉合成路线 (共 12 条)
反应条件
sodium perchlorate in 1,4-dioxane; water T=25°C; 45 h; pH 2.37; Title compound not separated from byproducts;
参考文献
Bushman, Daniel R.; Sayer, Jane M.; Boyd, Derek R.; Jerina, Donald M.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2688 - 2691
反应条件
silica gel T=110°C; 0.25 h; isomerization;
参考文献
Tetrahedron Letters, , vol. 27, # 36 p. 4253 - 4256
反应条件
sodium perchlorate in 1,4-dioxane; water T=25°C; 45 h; pH 2.37; Title compound not separated from byproducts;
参考文献
Bushman, Daniel R.; Sayer, Jane M.; Boyd, Derek R.; Jerina, Donald M.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2688 - 2691
反应条件
silica gel T=110°C; 0.25 h; isomerization;
参考文献
Tetrahedron Letters, , vol. 27, # 36 p. 4253 - 4256
反应条件
sodium hypochlorite; potassium phosphate; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane Ambient temperaturepH 8.6;
参考文献
Boyd, Derek R.; Davies, R. Jeremy H.; Hamilton, Lynne; McCullough, John J.; Porter, H. Patricia
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 9 p. 2189 - 2192
反应条件
sodium hypochlorite; potassium phosphate; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane Ambient temperaturepH 8.6;
参考文献
Boyd, Derek R.; Davies, R. Jeremy H.; Hamilton, Lynne; McCullough, John J.; Porter, H. Patricia
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 9 p. 2189 - 2192
反应条件
potassium deuteroxide; tert-BuOD; water-d2 T=40°C; 48 h;
参考文献
Agarwal, Shiv K.; Boyd, Derek R.; Davies, R. Jeremy H.; Hamilton, Lynne; Jerina, Donald M.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 1969 - 1974
反应条件
sodium perchlorate in 1,4-dioxane; water T=25°C; 45 h; pH 2.37; Title compound not separated from byproducts;
参考文献
Bushman, Daniel R.; Sayer, Jane M.; Boyd, Derek R.; Jerina, Donald M.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2688 - 2691
反应条件
potassium deuteroxide; tert-BuOD; water-d2
T=40°C; 48 h;
参考文献
Agarwal, Shiv K.; Boyd, Derek R.; Davies, R. Jeremy H.; Hamilton, Lynne; Jerina, Donald M.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 1969 - 1974
反应条件
sodium perchlorate in 1,4-dioxane; water
T=25°C; 45 h; pH 2.37; Title compound not separated from byproducts;
参考文献
Bushman, Daniel R.; Sayer, Jane M.; Boyd, Derek R.; Jerina, Donald M.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2688 - 2691