反应条件
1: tetrachloromethane; sodium azide; triphenylphosphine / N,N-dimethyl-formamide / 6 h / 90 °C
2: palladium 10 on activated carbon; hydrogen / methanol / 20 °C
3: pyridine / dichloromethane / 3 h / 0 - 20 °C
View Scheme
参考文献
El Kazzouli, Said; Griffon Du Bellay, Amaury; Berteina-Raboin, Sabine; Delagrange, Philippe; Caignard, Daniel-Henry; Guillaumet, Gerald
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 9 p. 4252 - 4257
