(±)-反式-1,3-二苯基烯丙基乙酸酯合成路线 （共 31 条）
反应条件
1.1: Mg / diethyl ether / Heating
1.2: 98 percent / diethyl ether / 20 °C
2.1: 90 percent / Et3N / CH2Cl2 / 20 °C
View Scheme
参考文献
Watson, Iain D. G.; Yudin, Andrei K.
Journal of the American Chemical Society, 2005 , vol. 127, # 49 p. 17516 - 17529
反应条件
1.1: Mg / diethyl ether / Heating
1.2: 98 percent / diethyl ether / 20 °C
2.1: 90 percent / Et3N / CH2Cl2 / 20 °C
View Scheme
参考文献
Watson, Iain D. G.; Yudin, Andrei K.
Journal of the American Chemical Society, 2005 , vol. 127, # 49 p. 17516 - 17529
反应条件
CuF2; potassium hydrogen difluoride; silver(I) acetate; palladium diacetate in acetone
T=85°C; Heck reaction; 5 h; chemoselective reaction;
参考文献
Su, Yijin; Jiao, Ning
Organic Letters, 2009 , vol. 11, # 14 p. 2980 - 2983
反应条件
1: sodium hydroxide / methanol; water / 5 - 25 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C
3: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 20 °C
View Scheme
参考文献
Yuan, Feng-Quan; Gao, Lian-Xun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 18 p. 5289 - 5291
反应条件
1: sodium hydroxide / methanol; water / 5 - 25 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C
3: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 20 °C
View Scheme
参考文献
Yuan, Feng-Quan; Gao, Lian-Xun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 18 p. 5289 - 5291
反应条件
1: NaBH4; CeCl3 / methanol
2: DMAP / diethyl ether
View Scheme
参考文献
Gotov, Battsengel; Toma, Stefan; Solcaniova, Eva; Cvengros, Jan
Tetrahedron, 2000 , vol. 56, # 4 p. 671 - 675
反应条件
1: Bromure de phenyl magnesium With lithium tetrachloromanganate(II) in tetrahydrofuran
0.75 h; cooling;
2: With chloro-trimethyl-silane in tetrahydrofuran
T=-10°C; 0.333333 h;
3: (2E)-1-(acetyloxy)-3-phenylprop-2-enyl acetate in tetrahydrofuran
T=-10°C; Further stages.;
参考文献
Deshmukh, Madhukar B.; Jadhav, Sunil D.; Kadam, Shashikant V.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 6 p. 989 - 994
反应条件
1: diethyl ether / 2 h / Heating
2: 78 percent / triethylamine; DMAP / diethyl ether / 20 °C
View Scheme
参考文献
Malkov; Baxendale; Mansfield; Kocovsky
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 10 p. 1234 - 1240
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
参考文献
Ruzziconi, Renzo; Santi, Claudio; Spizzichino, Sara
Tetrahedron Asymmetry, 2007 , vol. 18, # 14 p. 1742 - 1749
反应条件
1.) Et2O, 2.) pyridine; Yield given. Multistep reaction;
参考文献
Allen, Joanne V.; Coote, Steven J.; Dawson, Graham J.; Frost, Christopher G.; Martin, Christopher J.; Williams, Jonathon, M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 15 p. 2065 - 2072
