三甲基(1,2,3,4,5-五甲基环戊二烯基)硅烷合成路线 （共 7 条）
反应条件
in tetrahydrofuran T=0°C; 2 h;
参考文献
Llinas, Gerardo Hidalgo; Mena, Miguel; Palacios, Federico; Royo, Pascual; Serrano, Ricardo
Journal of Organometallic Chemistry, 1988 , vol. 340, p. 37 - 40
反应条件
T=150 - 160°C; 96 h;
参考文献
Jutzi, Peter; Saleske, Hartmut; Buehl, Dittmar; Grohe, Hildegard
Journal of Organometallic Chemistry, 1983 , vol. 252, # 1 p. 29 - 36
反应条件
in tetrahydrofuran T=-50 - 20°C; Title compound not separated from byproducts;
参考文献
Russian Chemical Bulletin, , vol. 53, # 10 p. 2182 - 2186
反应条件
in tetrahydrofuran T=-50 - 20°C; Title compound not separated from byproducts;
参考文献
Russian Chemical Bulletin, , vol. 53, # 10 p. 2182 - 2186
反应条件
Total yield 88 percent;
参考文献
Chemistry Letters, , p. 1309 - 1312
反应条件
in toluene under Ar atm. using Schlenk techniques; recrystd. from toluene/pentane;
参考文献
Kim, Youngjo; Han, Yonggyu; Hwang, Jeong-Wook; Kim, Myong Woon; Do, Youngkyu
Organometallics, 2002 , vol. 21, # 6 p. 1127 - 1135
反应条件
in dichloromethane
under Ar, dropwise addn. of a soln. of Me3SC5Me5 to a soln. of the B-compound at -40°C, stirring (room temp., 1 h);; fractionated distn.;
参考文献
Jutzi, Peter; Krato, Bruno; Hursthouse, Mike; Howes, Andrew J.
Chemische Berichte, 1987 , vol. 120, p. 565 - 574
