4-(吡啶-3-基氧基)苯甲酸甲酯合成路线 (共 3 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=135°C; 10 h;
参考文献
TARGEGEN, INC.
Patent: WO2006/24034 A1, 2006 ;
Location in patent: Page/Page column 84 ;
反应条件
potassium phosphate; 2-di-tert-butylphosphino-2',4',6'-tricyclohexyl-3,6-dimethoxybiphenyl in ethylene glycol dimethyl ether; toluene
T=80°C; 24 h; Inert atmosphere;
参考文献
Salvi, Luca; Davis, Nicole R.; Ali, Siraj Z.; Buchwald, Stephen L.
Organic Letters, 2012 , vol. 14, # 1 p. 170 - 173
反应条件
hydrazine in ethanol
24 h; Heating / reflux;
参考文献
TARGEGEN, INC.
Patent: WO2006/24034 A1, 2006 ;
Location in patent: Page/Page column 84-85 ;