potassium dihydrogenphosphate; Fremy’s salt in water; acetone
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2711 - 2715
1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 219 mg / CHCl3 / 144 h / Ambient temperature; in the dark
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 219 mg / CHCl3 / 144 h / Ambient temperature; in the dark
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
1: air / chromatography on SiO2
2: 219 mg / CHCl3 / 144 h / Ambient temperature; in the dark
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2711 - 2715
in chloroform
144 h; Ambient temperaturein the dark;
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
