in tetrahydrofuran LiSnMe3 added to PhSnEt3 in THF, stirred at 24°C for 1 h, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products isolated by preparative by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
in tetrahydrofuran NaSnMe3 added to PhSnEt3 in THF, stirred at 50°C for 30 min, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
in tetrahydrofuran KSnMe3 added to PhSnEt3 in THF, stirred at 50°C for 30 min, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
in N,N,N',N',N'',N''-hexamethylphosphoric triamide LiSnMe3 added to PhSnEt3 in HMPA, stirred at 24°C for 1 h, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
Ladenburg, A.
Ber. Dtsch. Chem. Ges., 1871 , vol. 4, p. 17 - 18
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Ladenburg, A.
Liebigs Annalen der Chemie, 1871 , vol. 159, p. 251 - 258
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.9, page 238 - 244
