in tetrahydrofuran
LiSnEt3 added to PhSnMe3 in THF, stirred at 50°C for 30 min, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Mochida, Kunio
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3299 - 3306
in toluene
byproducts: tetraphenylantimony chloride; mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampooule at room temp. for 24 h; crystals of Ph4SbCl filtered off, filtrate evapd., residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
Ladenburg, A.
Ber. Dtsch. Chem. Ges., 1871 , vol. 4, p. 17 - 18
Full Text Show Details
Ladenburg, A.
Liebigs Annalen der Chemie, 1871 , vol. 159, p. 251 - 258
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.9, page 238 - 244
