反应条件
1: 86 percent / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature
2: 50 percent / NaN(SiMe3)2 / tetrahydrofuran / 20 h / Ambient temperature
3: 89.3 percent / Et3N / CH2Cl2 / 32 h / 25 °C
4: 79 percent / 1.03M sec-BuLi / cyclohexane; tetrahydrofuran / -70 deg C, 3 h; RT, 2 h
5: 1.0M LiBHEt3 / tetrahydrofuran / -10 deg C to RT
View Scheme
参考文献
Meyers, Albert I.; Fray, Andrew H.
Bulletin de la Societe Chimique de France, 1997 , vol. 134, # 3-4 p. 283 - 298
