2-氯-3-氰吡啶-4-硼酸频哪酯合成路线 （共 2 条）
反应条件
magnesium sulfate in toluene T=20°C; 12 h;
参考文献
Cailly, Thomas; Fabis, Frederic; Bouillon, Alexandre; Lemaitre, Stephane; Sopkova, Jana; De Santos, Olivieira; Rault, Sylvain
Synlett, 2006 , # 1 art. no. G33905ST, p. 53 - 56
反应条件
1.1: 2,2,6,6-tetramethylpiperidine; n-BuLi / tetrahydrofuran / 0.5 h / -80 °C 1.2: tetrahydrofuran / -80 - 20 °C 2.1: aq. HCl / pH 6 3.1: 77 percent / MgSO4 / toluene / 12 h / 20 °C View Scheme
参考文献
Synlett, , # 1 art. no. G33905ST, p. 53 - 56
