反应条件
1: TsOH / methanol / 24 h / 50 °C
2: diisobutylaluminum hydride / CH2Cl2 / 1 h / -78 °C
3: pyridine / 1 h / 0 - 20 °C
4: sodium azide / dimethylformamide / 24 h / 50 °C
5: p-toluenesulfonic acid / methanol / 24 h / 50 °C
6: H2 / Lindlar catalyst / methanol / 12 h / 23 °C / 760 Torr
7: acetonitrile / 4 h
8: benzyltrimethylammonium dichloroiodate / tetrahydrofuran / 1.75 h / 60 °C
9: acetonitrile / 40 h / 35 °C
10: aq. HCl / methanol / 16 h / 23 °C
11: H2O / 4 h / 95 °C
View Scheme
参考文献
O'Malley, Daniel P.; Li, Ke; Maue, Michael; Zografos, Alexandros L.; Baran, Phil S.
Journal of the American Chemical Society, 2007 , vol. 129, # 15 p. 4762 - 4775
