(R)-(+)-1,2-癸二醇合成路线 （共 13 条）
反应条件
AD-mix-β in water; tert-butyl alcohol Sharpless Asymmetric Epoxidation;
参考文献
Weihrather, Joachim; Jauch, Johann
Synlett, 2013 , vol. 24, # 11 art. no. ST-2013-B0271-L, p. 1410 - 1414
反应条件
potassium dioxotetrahydroxoosmate(VI); potassium carbonate; dihydroquinidine 9-O-(9'-phenanthryl) ether hydrochloride; potassium hexacyanoferrate(III) in water; tert-butyl alcohol T=0°C; 18 h; enantioselective oxidation; further alkenes investigated; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 56, # 15 p. 4585 - 4588
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Kakeya, Hideaki; Sakai, Naoko; Sugai, Takeshi; Ohta, Hiromichi
Agricultural and Biological Chemistry, 1991 , vol. 55, # 7 p. 1877 - 1881
反应条件
1: 74 percent / pyridine / CH2Cl2 / -78 - 0 °C 2: aq. phosphate buffer / diisopropyl ether / 12 h / 10 °C / porcine pancreas lipase View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 10 p. 2977 - 2987
反应条件
phosphate buffer in di-isopropyl ether T=10°C; 12 h; porcine pancreas lipase; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 10 p. 2977 - 2987
反应条件
2: NaOMe / methanol / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 4, # 10 p. 2211 - 2218
反应条件
potassium carbonate in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 10 p. 2977 - 2987
反应条件
2: K2CO3 / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 10 p. 2977 - 2987
反应条件
1: 1.) 0.1M phosphate buffer / 1.) Rhodococcus botanica ATCC 21197, 30 deg C, 9 h 2: 82 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 55, # 7 p. 1877 - 1881
反应条件
sodium phosphate buffer T=10°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 36, # 36 p. 6499 - 6502
