trifluoroacetic acid in dichloromethane T=20°C; 12 h;
参考文献
Jones, Mathew W.; Strickland, Rachel A.; Schumacher, Felix F.; Caddick, Stephen; Baker, James. R.; Gibson, Matthew I.; Haddleton, David M.
Journal of the American Chemical Society, 2012 , vol. 134, # 3 p. 1847 - 1852
Multi-step reaction with 2 steps 1.1: triethylamine / N,N-dimethyl-formamide / 0 - 20 °C2.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C2.2: 0 - 20 °C
参考文献
Jones, Mathew W.; Strickland, Rachel A.; Schumacher, Felix F.; Caddick, Stephen; Baker, James. R.; Gibson, Matthew I.; Haddleton, David M. Journal of the American Chemical Society, 2012 , vol. 134, # 3 p. 1847 - 1852
