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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87861-97-0
合成路线
（共 21 条）
87861-97-0
→
反应条件
1015-89-0
6(5H)-菲啶酮
反应条件
trifluoroacetic acid T=100°C; 24 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Sferrazza, Alessio
Synthesis, 2008 , # 5 p. 729 - 738
87861-97-0
→
反应条件
15679-03-5
6-氯菲啶
反应条件
trichlorophosphate T=190°C;
参考文献
Mitsuhashi
Yakugaku Zasshi, 1943 , vol. 63, p. 177,181
Chem.Abstr., 1951 , p. 628
82082-50-6
N-苄基-2-溴苯甲酰胺
→
反应条件
87861-97-0
+
3173-56-6
异氰酸苄酯
反应条件
[2-(8-methoxynaphthalen-1-yl)phenyl]diphenylphosphane; caesium carbonate; palladium diacetate in 1,4-dioxane T=100°C; 24 h;
参考文献
Furuta, Takumi; Kitamura, Yuki; Hashimoto, Ayano; Fujii, Satoshi; Tanaka, Kiyoshi; Kan, Toshiyuki
Organic Letters, 2007 , vol. 9, # 2 p. 183 - 186
82082-50-6
N-苄基-2-溴苯甲酰胺
→
反应条件
87861-97-0
反应条件
bis-triphenylphosphine-palladium(II) chloride; caesium carbonate in tetrahydrofuran T=60°C; Inert atmosphere;
参考文献
Donati, Ludovic; Michel, Sylvie; Tillequin, Francois; Poree, Francois-Hugues
Organic Letters, 2010 , vol. 12, # 1 p. 156 - 158
1028196-25-9
→
反应条件
87861-97-0
反应条件
potassium carbonate; 1,2-bis-(diphenylphosphino)ethane; palladium diacetate in N,N-dimethyl-formamide T=100°C; 0.5 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Sferrazza, Alessio
Synthesis, 2008 , # 5 p. 729 - 738
1253736-34-3
→
反应条件
87861-97-0
反应条件
copper(I) thiophene-2-carboxylate in N,N-dimethyl-formamide T=200°C; Ullmann type reaction; Microwave irradiation;
参考文献
Boonya-Udtayan, Sasiwadee; Yotapan, Nattawut; Woo, Christina; Bruns, Carson J.; Ruchirawat, Somsak; Thasana, Nopporn
Chemistry - An Asian Journal, 2010 , vol. 5, # 9 p. 2113 - 2123
7506-50-5
+
121-46-0
2,5-降冰片二烯
→
反应条件
87861-97-0
反应条件
palladium diacetate; caesium carbonate; [(t-Bu)3PH]BF4 in N,N-dimethyl-formamide T=130°C; Inert atmosphere;
参考文献
Thansandote, Praew; Hulcoop, David G.; Langer, Michael; Lautens, Mark
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1673 - 1678
141-32-2
丙烯酸丁酯
+
52648-48-3
→
反应条件
229-87-8
菲啶
+
87861-97-0
反应条件
oxygen; copper diacetate; palladium dichloride in N,N-dimethyl acetamide T=120°C; P=760.051 Torr; 48 h;
参考文献
Liu, Yan-Yun; Song, Ren-Jie; Wu, Cui-Yan; Gong, Lu-Bin; Hu, Ming; Wang, Zhi-Qiang; Xie, Ye-Xiang; Li, Jin-Heng
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 347 - 353
82082-50-6
N-苄基-2-溴苯甲酰胺
→
反应条件
1202160-24-4
+
87861-97-0
反应条件
bis-triphenylphosphine-palladium(II) chloride; caesium carbonate in 1,4-dioxane T=100°C; Inert atmosphere;
参考文献
Donati, Ludovic; Michel, Sylvie; Tillequin, Francois; Poree, Francois-Hugues
Organic Letters, 2010 , vol. 12, # 1 p. 156 - 158
82082-50-6
N-苄基-2-溴苯甲酰胺
+
88284-48-4
2-(三甲基硅)苯基三氟甲烷磺酸盐
→
反应条件
87861-97-0
反应条件
palladium diacetate; sodium carbonate; cesium fluoride; bis(1,1-diphenylphosphino)methane in toluene; acetonitrile T=20 - 110°C;
参考文献
Lu, Chun; Dubrovskiy, Anton V.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8648 - 8656
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